ftir-8400s manual

See our User Agreement and Privacy Policy.If you continue browsing the site, you agree to the use of cookies on this website. See our Privacy Policy and User Agreement for details.If you wish to opt out, please close your SlideShare account. Learn more. You can change your ad preferences anytime. Shimadzu was the first company to offer dynamic alignment as a standard feature in an affordable FTIRFTIR-8400S is combined with the IRsolution - a 32 bit high performance FTIR software - to analyze yourT h e I R s o l u t i o n A dva n t ag eCable Add.:SHIMADZU TOKYO Phone: (55)11-3611-1688 Fax. (55)11-3611-2209Phone: 1(410)381-1227 Fax. 1(410)381-1222 Toll Free: 1(800)477-1227 Phone: (852)2375-4979 Fax. (852)2199-7438. SHIMADZU EUROPA GmbH SHIMADZU INTERNATIONAL TRADING (SHANGHAI) Co., LTD. SHANGHAI OFFICE. Albert-Hahn-Strasse 6-10, 47269 Duisburg, F.R. Germany Phone: 49(203)7687-0 Fax. 49(203)766625 24th Floor, Shanghai Xin Hualian Building, No.755 Huaihai Zhong Lu, Shanghai, ChinaPhone: 65-6778-6280 Fax. 65-6779-2935 Istanbul, MoscowPhone: 61(2)9684-4200 Fax. 61(2)9684-4055Now customize the name of a clipboard to store your clips. The connection's current state is open. Please review the stack trace for more information about the error and where it originated in the code.The connection's current state is open. Source Error: Information regarding the origin and location of the exception can be identified using the exception stack trace below. The IR source mirror seemed ” The item may have some signs of cosmetic wear, but is fully operational and functions as intended. This item may be a floor model or store return that has been used. See the seller’s listing for full details and description of any imperfections. The IR source mirror seemed to be hazed over and The entrance window is a little dirty (can be cleaned easily). You will need a 68 pin SCSI connection to use this and a computer as neither was included when the item was purchased.

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IRPrestige-21, IRAffinity-1 and FTIR-8400S (IRsolution model) can be controlled from the FTIR-8400S. Shimadzu. Fourier Transform. Infrared Spectrophotometer. C103-E063F On-screen instructions for easy operation. Laptop PC control is available FTIR 8400s Catalogue - Free download as PDF File (.pdf), Text File (.txt) or read online for free. Shimadzu was the first company to offer dynamic alignment as a standard FTIR operators will love the quick-start function that prompts the user through every action. Keeler Vantage Plus Ophthalmoscope - Service Manual. FTIR-8400S is combined with the IRsolution - a 32 bit high performance FTIR software - to analyze your samples easily and securely. Dynamic alignment ensures reproducibility by maintaining optimum alignment Highly precise control of the moving mirror is required to stabilize the interferogram of the FTIR instrument. The FTIR-8400S includes the patented FJS system - very smooth and precise moving mirror unit - and the Dynamic Alignment system to optimize and stabilize the inter-ferometer unit. FTIR-8400S requires only a short stabilization time and is very secure. Dynamic Alignment (Patented) This System monitors the interferometer condition of He-Ne laser and compares it with that of optimized conditions. Any detected discrepancies by DSP system are corrected by automatic alignment of the piezo actuators at the fixed mirror. The Dynamic Alignment Advantage Optimal interferometer alignment is maintained automatically for continuous optimization and exceptional reproducibility. The Simplicity Advantage New FTIR operators will love the quick-start function that prompts the user through every action from setting scan parameters and acquiring the spectrum, to detecting peaks and printing. Notify me of new posts via email. Learn how your comment data is processed. To find out more, including how to control cookies, see here. If you continue browsing the site, you agree to the use of cookies on this website.

With state-of-the-art technology, the Shimadzu dynamic alignment system continuously maintains optimal alignment during data acquisition, ensuring consistently reproducible spectra without the need for tedious mechanical adjustments. FTIR-8400S is combined with the IRsolution - a 32 bit high performance FTIR software - to analyze your samples easily and securely. The Dynamic Alignment Advantage Optimal interferometer alignment is maintained automatically for continuous optimization and exceptional reproducibility. The Simplicity Advantage New FTIR operators will love the quick-start function that prompts the user through every action from setting scan parameters and acquiring the spectrum, to detecting peaks and printing.Dynamic alignment ensures reproducibility by maintaining optimum alignment Highly precise control of the moving mirror is required to stabilize the interferogram of the FTIR instrument. The FTIR-8400S includes the patented FJS system - very smooth and precise moving mirror unit - and the Dynamic Alignment system to optimize and stabilize the interferometer unit. FTIR-8400S requires only a short stabilization time and is very secure. He-Ne laser Piezo-actuator Signal amplifier Fixed mirror DSP Dynamic Alignment (Patented) This System monitors the interferometer condition of He- Ne laser and compares it with that of optimized conditions. Any detected discrepancies by DSP system are corrected by automatic alignment of the piezo actuators at the fixed mirror. The standard features include auto aperture, auto focusing, auto X-Y-Z stage movement and auto centering, as well as the transmittance and reflectance modes, and the on-board video-camera. Meet all your sampling requirements with such convenient options as grazing angle objectives, various ATR objectives and mapping software.

” Our location is: 826 Columbia Ave. Millville, NJ 08332. Any questions, please call (856) 300-5138 between 10:00PM and 7:00 PM EST with the item number and your user ID and we will be happy to assist you. Thanks!:). Discover everything Scribd has to offer, including books and audiobooks from major publishers. Start Free Trial Cancel anytime. Report this Document Download Now Save Save FTIR 8400s Catalogue For Later 0 ratings 0% found this document useful (0 votes) 647 views 2 pages FTIR 8400s Catalogue Uploaded by fierywin Description: Full description Save Save FTIR 8400s Catalogue For Later 0% 0% found this document useful, Mark this document as useful 0% 0% found this document not useful, Mark this document as not useful Embed Share Print Download Now Jump to Page You are on page 1 of 2 Search inside document Browse Books Site Directory Site Language: English Change Language English Change Language. We also share information about your use of our Website with our group companies, distributors and analytics partners.Please confirm that JavaScript is enabled in your browser. These are utilized in a wide range of structural analysis or non-destructive measurement applications, such as to qualify the location of defects on IC chips and other small parts in electronics, electrical, and semiconductor industries, to qualify pharmaceuticals based on the Japanese Pharmacopoeia, to identify vehicles from paint fragments left at crime scenes, or to verify starting materials on beads as a pre-synthesis study in combinatorial chemistry. This sensitivity combined with the LabSolutions IR Contaminant Analysis Macro enables easier, quicker and more accurate analysis of small samples. Labor-saving macros provide for a higher level of automation and improved work efficiency. Not for use in diagnostic procedures. Please contact us to check the availability of these products in your country.

The path length is selected according to concentration of the gas. Samples are clamped to the prism to ensure contact. For samples with high refractive indices, the Ge prism is suitable. For hard samples, the diamond prism is preferred. With the ATR correction available within the IRsolution software, ATR spectra is converted into a normal transmittance spectra. Another method for these sample types, involves scratching the surface of the sample and measuring with a diffuse reflectance accessory. A large contact area results in good sensitivity. The ZnSe prism is standard in most accessories. A Ge prisms is available for high refractive index samples. The measuring light is reflected through the prism 10 times. The sample is clamped firmly to the prism to ensure contact with an attached clamp and easily adjustable clamp pressure. This accessory is suitable for liquid, solids, powders, films, and a variety of other sample types. The ZnSe prism is standard. A Ge prism is available for high refractive index samples. The sample can be easily clamped to prism with the attached clamp with adjustable pressure. For hard samples, the Diamond MIRacle with diamond prism is available. Single Bounce ATR with a 2mm diameter diamond prism. This accessory is good for measuring hard samples that may damage other prism types. It is also suitable for liquid, solids, powders, films, and a variety of other sample types. The System I (High Pressure Device Type) allows the sample to contact the prism easily with the attached clamp and adjustable pressure. The System H (ViewIR Type) allows the sample to be visually observed while clamping. The powder of the sample on the emery paper is directly analyzed with a Diffuse Reflectance Accessory. 7 8 Versatility Versatility 2 For coating films on metals or resins For coatings, Reflectance is the measurement method is a choice. Selection of Specular Reflection or Reflection absorption method is dependent on the thickness of the coating sample.

Universal sampling with a diamond ATR Left Side: System I (High Pressure Device type) Right Side: System H(ViewIR type) Infrared spectrum of diphenhydramin hydrochloride(powder sample) measured with DuraSampllR2A (ATR-corrected spectrum) The DuraSampllR2A has two types of diamond prism, a diamond prism supported by a ZnSe lens and a diamond prism supported by a KRS-5 lens. The ZnSe type can measure up to around 600cm -1. On the other hand, the KRS-5 type can measure up to around 400cm -1. The infrared spectrum of diphenhydramin hydrochloride measured with the diamond prism supported by a KRS-5 lens is shown above. The KRS-5 type can give the infrared spectrum without noise up to 400cm -1. Plastics, rubbers, files and liquid samples can be measured with the DuraSampllR2A. 5 6 Versatility Versatility 2 For Liquid samples For measuring liquid samples, demountable or sealed liquid cells may be used. Additionally, the ATR (Attenuated Total Reflectance) accessories are also convenient. To measure liquids with ATR, sample preparation is as simple as dispensing the liquid onto the prism of the accessory. The ATR correction program in the IRsolution software converts the measured ATR spectrum into a normal transmittance measurement by correcting for depth penetration differences. The ZnSe prism is standard in most accessories. This accessory is suitable for liquid, solids, powders, films, and a variety of other sample types. The ZnSe prism is standard. A Ge prism is available for high refractive index samples. For powder samples For measuring powder samples, conventional KBr pellet methods may be used. The Diffuse reflectance method is also convenient and requires less sample preparation. In the Diffuse reflectance method, the sample is mixed with KBr powder and then measured, there is no need for making a pellet. Single Bounce ATR accessories may also be used for powder samples in some cases. For gases Various gas cells are available for gas sample measurement.

The IRsolution software has many functions ranging from Peak detection, spectral subtraction, Kubelka-Munk conversion and ATR correction functions to optional Spectrum searching and Quantitation. The results of data processing can be imported into Word Processing and Spread Sheet software applications. Pesk Picking Spectrum Search Quantitation Quantitation In addition to multi-point calibration curve methods, the IRsolution software offers MLR (Multi Linear Regression) and optional PLS (Partial Least Squares) analysis that is useful for NIR measurements. Spectrum Search The IRsolution software allows the creation of user libraries from acquired spectra, and spectral searching of user and commercial libraries. Report Generator Data is not useful unless you can get the results in the desired format. The IRsolution software includes a powerful report generator with customized layout features. With the Report Generator, you can create reusable print templates using any data including the spectrum, calibration curve, quantitation results and peak pick tables. You can set the thickness and color of the graph lines as well as the font size. Annotations may be attached on the graph to comment on the results. The print layout can be saved as a template file for later use, ensuring accurate repeat reporting. 11 12 Validation Reliability Reliability 1 FTIR-8400S has many features on hardware and within the software that improve reliability. Measurement conditions of the FTIR-8400S are constantly monitored and may be reported at anytime. IRsolution is complied to GLP and FDA 21 CFR Part 11. This validation program checks the performance of the FTIR-8400S using a polystyrene film and creates a report upon completion. History log of data processing. Software security by User name and Password By requiring a user name and password upon startup of the IRsolution software, security can enhanced by restricting the functions or methods for the particular user within a user group.

An administrator can restrict the functionality that is available within IRsolution to each particular user and can control all the user rights. The logon information is recorded into a log-file with the date, time and user name. Data Preservation, Operation Logging, Audit-trail of the instrument Spectra that are obtained by the IRsolution software are stored in a Container file that includes with scan parameters, background and the original interferogram. When a data manipulation is performed, the processed data is added to the file along with date and time of processing, user name and the manipulation method. The original data is preserved - not overwritten. This file can be displayed and is write-protected by the IRsolution software for security. The electronic signature is also supported for FDA 21 CFR Part 11 compliance.Operation Log 12 13 Hardware Reliability Reliability 2 The Interferometer is one of the most important parts of the FTIR. For accurate data collection, the interferometer must scan with high precision. The FTIR-8400S includes the Patented FJS system which scans the moving mirror with a smooth and stable mechanism. The optimization and stabilization of the FTIR-8400S interferometer by Dynamic Alignment system ensures consistent and repeatable results. Since the beam splitter within the interferometer is susceptible to moisture, the optical system of the FTIR-8400S is sealed and desiccated. Protection of the Interferometer and Atmosphere Correction The Interferometer is one of the most important parts of the FTIR. The FTIR-8400S has 3 features to stabilize the interferometer and to protect the beam splitter. 1. Sealed optical system to create closed environment 2. Anti Humidity Beam Splitter coating to provide extra protection 3.

Samples are placed on the top of the accessory with the measurement side down. The specular reflectance spectra can convert into a transmittance spectra with Kramers-Kronig conversion in the IRsolution software. Analysis of nm thick thin films is possible. The optional GPR-8000 polarizer allows for higher sensitivity measurement. When a polarized light beam is incident on a metal substrate, the phase of the light is changed. In vertical polarization, the vectors of the polarized light are opposite to each other, and hence no stationary waves are produced. In parallel polarization, the the vectors of the polarized light meet at the point to produce stationary waves, which enhances the sensitivity of the measurement. Accessory for automated analysis Various automation accessories, are available to provide efficient analysis of large numbers of samples. The holder is designed for 13mm diameter KBr pellets and optional film-holder or cell plates for Nujol mulls are also available. The ASC-8000T can be easily controlled by the IRsolution software. The DRS-8010ASC accepts up to 24 samples. The DRS-8010ASC can be easily controlled by IRsolution software. Infrared spectrum of lactose Infrared spectrum of lactose measured with the DRS-8010ASC automatic diffuse reflectance accessory (Kubelka-Munk concerted spectrum) 8 9 Versatility 3 Space Efficient Laptop PC Control A unique laptop PC rack option (note1) reduces the system footprint to just 630mm (W) by 592mm (D), and the height to only 530mm. Process your data anywhere with this portable PC option. (note1) Rack accommodates 13.3 inch laptop PC. (note2) Microscope-equipped systems require desktop PC. (note3) Special SCSI interface for laptop PCs is required. In either case, procedures can be simplified by standard Easy-Scan program, all procedures including the setting of measurement parameters, analysis of the sample, data processing, saving, and printing the results are performed with one click operation.

The IRsolution software is equipped with an Easy-Scan program. This macro program takes the user step by step through the entire analysis from spectrum measurement, peak detection, printout and saving of the result data. On screen instructions guide the operator ever step of the way. This feature allows for a decrease in the learning curve for operating the IRsolution and the FTIR-8400S. Scan Parameter Setting BKG Measurement Peak Detection 9 10 Software IRsolution IRsolution software provides windows based 32bit software control for the FTIR-8400S. With IRsolution, operations for FTIR analysis can be performed easily and quickly using dedicated analysis screens Spectrum measurement Data display and comparison to other spectra Data processing, quantitation and spectral searching Report Generation As the operation progresses, the IRsolution software automatically advances into the optimum mode. Optional software such as PLS quantitation modules are available for increased versatility. You can quickly access the many useful functions of IRsolution by customizing the User Interface of software. Measurement and Status Monitor In the measurement menu of IRsolution, all measurement start buttons and dialogs to set the analysis parameters are integrated for easy operation. All measurement parameters are arranged into four dialog screens that are easily viewed. One click operation will start the analysis. During measurement, a real time spectrum is displayed on screen. The hardware settings are displayed on the status monitor screen. Status Monitor View Mode After the data is acquired, you can use the View Mode to zoom in on certain areas or compare with other spectra. 10 11 Data Manipulation, Quantitation and Spectrum Search After the data acquisition has been completed, you can extract a variety of specific information from measured spectrum.

Desiccated interferometer to remove moisture by Desiccants He-Ne laser Moving mirror Fixed mirror BS Colimator mirror Light sourse The Atmosphere Correction Function easily compensates for the influences of water vapor and carbon dioxide on your data. You can easily get beautiful spectra with the FTIR-8400S even if the sample has peaks which are overlap with water vapor around cm -1 or cm -1. Laser detector Sealing case Sample position KRS-5 window Condensing mirror Detector Elimination of influences of CO2 and H2O by Atmosphere Correction Blue: Spectrum Before Atmosphere Correction Red: Spectrum After Atmosphere Correction 13 14 Optional Software Optional Software Wide varieties of optional software to enhance IRsolution capabilities Powerful 32-bit Windows based software - IRsolution - has various optional software modules to enhance its performance: IRsolution Agent Mapping software - AIM-MAP (for the AIM-8800 Microscope) PLS quantitation software Curvefitting (Peak split) software PharmaReport Program note) Macro Platform IRsolution includes a wide selection of data manipulation operations which include: spectral subtraction and Kubelka-Munk conversion; Variety of Quantitation operations - Multi-point Method and Multiple Linear Regression (MLR) method; as well as Spectral search functions. The optional software for IRsolution expands the application capabilities of IRPrestige-21.IRsolution Agent software consists of a database function and a data registration function from IRsolution to IRsolution Agent, as well as electronic signature capabilities. Mapping conditions such as Mapping area, Scan intervals, Background position and etc.You can operate the AIM microscope and AIM-MAP through simple point and click operations. AIM-MAP has 3 types of mapping modes - Area mapping, Line mapping and Random mapping. IRsolution mapping has various data manipulation functions such as extracting a spectrum from mapped data or reprocessing functional-group mapping.

The mapped data can be shown as 3D bird's-eye view, counter plot or spectral overlay mode. IRsolution has PLS I and PLS II method for PLS quantitation. Curve fitting (Peak split) software separates IR bands to individual component peaks. This software is good for many applications such as analysis of peak with hydrogen bond influences, and analysis of hidden peaks overlapped with other peaks. Component peaks and a synthesized peak are displayed to evaluate the separation. Curve fitting (Peak split) result of peak ( cm -1 ) of ABS resin spectrum. The program conducts the following calculations and comparisons: Calculates the discrepancy in the peak wavenumbers of the sample being checked and the reference previously registered. Calculates the peak intensity ratio at several designated evaluation peaks for comparison between the sample and reference. In addition to the functions above, it is also possible to detect and print the previously designated peaks only, and to print out the spectra of the measured sample and the reference side by side. Dimensions With desktop PC (Unit: mm) With laptop PC using rack (Unit: mm) (note5) Dimensions for PC and Printer depend on models. JQA-0376 Founded in 1875, Shimadzu Corporation, a leader in the development of advanced technologies, has a distinguished history of innovation built on the foundation of contributing to society through science and technology. We maintain a global network of sales, service, technical support and applications centers on six continents, and have established long-term relationships with a host of highly trained distributors located in over 100 countries. For information about Shimadzu, and to contact your local office, please visit our Web site at SHIMADZU CORPORATION. International Marketing Division 3. Kanda-Nishikicho 1-chome, Chiyoda-ku, Tokyo, Japan Phone: 81(3) Fax. 81(3) URL The contents of this brochure are subject to change without notice.

Printed in Japan ATD I N T R O D U C T I O N FT-IR stands for Fourier Transform InfraRed, the preferred method of infrared spectroscopy. In infrared spectroscopy, Dispersive IR Spectroscopy This will enable PC control. Push the F4 Button 2) Log into the UV-VIS software with your username and password. 3) After Joe Van Gompel, PhD The electromagnetic The haze-gard i quantifies the visual perception All information contained in this publication is believed to be correct and complete. Thermo Electron Corporation shall not be liable Presentation Materials Richard Koops VSL Dutch Metrology Institute Delft You will need these skills to RotatIR Automated Rotating Sample Stage Accessory All information contained in this publication is believed No Turn on the Systems PC Switch Turn on Main Power Switch Yes Turn on the laser main power switch and turn Size and Edge Detection APPLICATIONS The EE-SX199 detects the absence or presence of labels (see Bar Code Printer illustration at right). Alluxa Engineering Staff Alluxa Engineering Staff December 2012 Specifying Advanced Plasma Deposited Hard Coated Optical Bandpass and Dichroic Filters. Introduction The SpectraTec II Ultraviolet-Visible MAS 40 Mini-Array Spectrometer.These advances in coating technology From cell phone cameras to space telescopes, driverless Plymouth, UK 15 17 February 2011.Claude Bernard (1813-1878) OBJECTIVES To examine the The precision and accuracy of a This CNC controlled machine features fast, simple programming coupled with high operating speeds to meet today s varied production requirements. Designed for When you specify a high resolution, Closed books, notes, etc. No electronic device except a calculator. No electronic device except a calculator. NAME: (all questions with equal weight) 1.

If the distance between two point charges is tripled, the This journal is The Royal Society of Chemistry 2014 Supporting Information Prussian blue nanoparticles for laser-induced photothermal therapy of In this lab you will use a spectrophotometer To use this website, you must agree to our Privacy Policy, including cookie policy.